SRF2019 - List of Authors (Bate, C.)

Paper	Title	Page
MOP023	Nitrogen Infusion Sample R&D at DESY	77
SUSP002	use link to see paper's listing under its alternate paper code
	C. Bate, A. Dangwal Pandey, A. Ermakov, B. Foster, T.F. Keller, D. Reschke, J. Schaffran, S. Sievers, N. Walker, H. Weise, M. Wenskat DESY, Hamburg, Germany W. Hillert University of Hamburg, Institut für Experimentalphysik, Hamburg, Germany G.D.L. Semione, V. Vonk DESY Nanolab, FS-NL, Hamburg, Germany A. Stierle University of Hamburg, Hamburg, Germany
	The European XFEL continuous wave upgrade requires cavities with reduced surface resistance (high Q-values) for high duty cycle while maintaining high accelerating gradient for short-pulse operation. A possible way to meet the requirements is the so-called nitrogen infusion procedure. However, a fundamental understanding and a theoretical model of this method are still missing. The approach shown here is based on sample R&D, with the goal to identify key parameters of the process and establish a stable, reproducible recipe. To understand the underlying processes of the surface evolution, which gives improved cavity performance, advanced surface analysis techniques (e.g. SEM/EDX, TEM, XPS, TOF-SIMS) are utilized. Additionally, a small furnace just for samples was set up to change and explore the parameter space of the infusion recipe. Results of these analyses, their implications for the cavity R&D and next steps are presented.
	Poster MOP023 [3.759 MB]
DOI •	reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-MOP023
About •	paper received ※ 23 June 2019 paper accepted ※ 30 June 2019 issue date ※ 14 August 2019
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MOP024	Vacancy-Hydrogen Dynamics in Samples During Low Temperature Baking	83
	M. Wenskat, C. Bate, D. Reschke, H. Weise DESY, Hamburg, Germany C. Bate University of Hamburg, Hamburg, Germany M. Butterling, E. Hirschmann, M.O. Liedke, A. Wagner HZDR, Dresden, Germany J. Cizek Charles University, Prague, Czech Republic
	Funding: This work was supported by the Helmholtz Association within the topic Accelerator Research and Development (ARD) of the Matter and Technologies (MT) Program and by the BMBF under the research grant 05H18GURB1. The recent discovery of a modified low temperature baking process lead to a reduction of surface losses and an increase of the accelerating gradient of TESLA shape cavities. The hypothesis linking the accelerator performance and the treatment is the suppression of lossy nanohydrides via defect trapping, with vacancy-hydrogen complexes forming at the lower temperatures. Utilizing Doppler broadening Positron Annihilation Spectroscopy and Positron Annihilation Lifetime Spectroscopy samples made from European XFEL niobium sheets and cavity cut-outs were investigated. The evolution of vacancies, hydrogen and their interaction at different temperature levels have been studied during in-situ annealing. Measurements of niobium samples and a correlation between RF, material properties, and V-H distribution in cavity cut-outs has been done.
	Poster MOP024 [1.087 MB]
DOI •	reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-MOP024
About •	paper received ※ 20 June 2019 paper accepted ※ 30 June 2019 issue date ※ 14 August 2019
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MOP025	Cavity Cut-out Studies of a 1.3 GHz Single-cell Cavity After a Failed Nitrogen Infusion Process	87
	M. Wenskat, C. Bate, T.F. Keller, D. Reschke DESY, Hamburg, Germany C. Bate University of Hamburg, Hamburg, Germany A. Jeromin DESY Nanolab, FS-NL, Hamburg, Germany J. Knobloch, F. Kramer, O. Kugeler, J.M. Köszegi HZB, Berlin, Germany J. Knobloch University of Siegen, Siegen, Germany
	Funding: This work was supported by the Helmholtz Association within the topic Accelerator Research and Development (ARD) of the Matter and Technologies (MT) Program and by the BMBF under the research grant 05H18GURB1. R&D on the nitrogen infusion process at DESY produced at the beginning a series of 1.3 GHz single-cell cavities which have shown severe deterioration in the vertical cold test which was completely unexpected and could not be explained. To investigate the reason for the deterioration, one of those cavities was optically inspected and a T- and H-Map test was done in collaboration with HZB. Together with 2nd Sound data, regions of interests were identified and cut from the cavity. Subsequent surface analysis techniques (SEM/EDX, SIMS, PIXE, EBSD, DB-PAS, PALS, XPS) were applied in order to identify the reason for the deterioration. Especially the differences between hot and cold spots as well as quench spots identified by T-Mapping were investigated.
	Poster MOP025 [0.975 MB]
DOI •	reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-MOP025
About •	paper received ※ 20 June 2019 paper accepted ※ 29 June 2019 issue date ※ 14 August 2019
Export •	reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

TUP099	Particulate Sampling and Analysis During Refurbishment of Prototype European XFEL Cryomodule	701
	N. Krupka, C. Bate, D. Reschke, S. Saegebarth, M. Schalwat, P. Schilling, S. Sievers DESY, Hamburg, Germany
	Funding: This work was supported by the Helmholtz Association within the topic Accelerator Research and Development (ARD) of the Matter and Tech-nologies (MT) Program. The cryomodule PXFEL3₁ is one of three prototype cryomodules for the European XFEL. In preparation of the series module assembly it was used for the qualification of infrastructure and personnel at CEA Saclay. After transport and tests at DESY the cryomodule was stored for several years. Last year we decided to refurbish this module with new cavities for the installation in the FLASH accelerator. During the disassembly of the cavity string in the clean room at DESY we took several particulate samples for analysis. Optical and laser optical microscopy give us an insight on the quantity and type of the particulates. We expect to get hints where the particulates come from and how they are transported through the cavity string during transport and operation.
	Poster TUP099 [2.599 MB]
DOI •	reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-TUP099
About •	paper received ※ 23 June 2019 paper accepted ※ 03 July 2019 issue date ※ 14 August 2019
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TUFUA6	Surface Analysis of Niobium After Thermal/Gas Treatments via Samples - Review
	A. Dangwal Pandey, T.F. Keller, H. Noei, D. Reschke, J. Schaffran, G.D.L. Semione, V. Vonk, H. Weise, M. Wenskat DESY, Hamburg, Germany C. Bate, A. Stierle University of Hamburg, Hamburg, Germany
	Thermal treatments of SRF Nb cavities - including the well-established 120°C bake and the recently reported N-infusion - are shown to improve the cavity performance significantly; however, the underlying physical phenomenon is not fully understood. A short review will be presented on surface characterization of niobium material subjected to various thermal and gas exposure protocols and how the findings correlate with observed SRF properties. Moreover, recent results obtained on single-crystal Nb samples - heated in different vacuum environments and characterised by means of X-ray photoelectron spectroscopy and grazing-incidence X-ray diffraction, electron microscopy, energy dispersive X-ray spectroscopy and time-of-flight secondary ion mass spectroscopy will be discussed.
	Slides TUFUA6 [6.968 MB]
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Paper

Title

Page

MOP023

Nitrogen Infusion Sample R&D at DESY

77

SUSP002

use link to see paper's listing under its alternate paper code

C. Bate, A. Dangwal Pandey, A. Ermakov, B. Foster, T.F. Keller, D. Reschke, J. Schaffran, S. Sievers, N. Walker, H. Weise, M. Wenskat
DESY, Hamburg, Germany
W. Hillert
University of Hamburg, Institut für Experimentalphysik, Hamburg, Germany
G.D.L. Semione, V. Vonk
DESY Nanolab, FS-NL, Hamburg, Germany
A. Stierle
University of Hamburg, Hamburg, Germany

The European XFEL continuous wave upgrade requires cavities with reduced surface resistance (high Q-values) for high duty cycle while maintaining high accelerating gradient for short-pulse operation. A possible way to meet the requirements is the so-called nitrogen infusion procedure. However, a fundamental understanding and a theoretical model of this method are still missing. The approach shown here is based on sample R&D, with the goal to identify key parameters of the process and establish a stable, reproducible recipe. To understand the underlying processes of the surface evolution, which gives improved cavity performance, advanced surface analysis techniques (e.g. SEM/EDX, TEM, XPS, TOF-SIMS) are utilized. Additionally, a small furnace just for samples was set up to change and explore the parameter space of the infusion recipe. Results of these analyses, their implications for the cavity R&D and next steps are presented.

Poster MOP023 [3.759 MB]

DOI •

reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-MOP023

About •

paper received ※ 23 June 2019 paper accepted ※ 30 June 2019 issue date ※ 14 August 2019

Export •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

MOP024

Vacancy-Hydrogen Dynamics in Samples During Low Temperature Baking

83

M. Wenskat, C. Bate, D. Reschke, H. Weise
DESY, Hamburg, Germany
C. Bate
University of Hamburg, Hamburg, Germany
M. Butterling, E. Hirschmann, M.O. Liedke, A. Wagner
HZDR, Dresden, Germany
J. Cizek
Charles University, Prague, Czech Republic

Funding: This work was supported by the Helmholtz Association within the topic Accelerator Research and Development (ARD) of the Matter and Technologies (MT) Program and by the BMBF under the research grant 05H18GURB1.
The recent discovery of a modified low temperature baking process lead to a reduction of surface losses and an increase of the accelerating gradient of TESLA shape cavities. The hypothesis linking the accelerator performance and the treatment is the suppression of lossy nanohydrides via defect trapping, with vacancy-hydrogen complexes forming at the lower temperatures. Utilizing Doppler broadening Positron Annihilation Spectroscopy and Positron Annihilation Lifetime Spectroscopy samples made from European XFEL niobium sheets and cavity cut-outs were investigated. The evolution of vacancies, hydrogen and their interaction at different temperature levels have been studied during in-situ annealing. Measurements of niobium samples and a correlation between RF, material properties, and V-H distribution in cavity cut-outs has been done.

Poster MOP024 [1.087 MB]

DOI •

reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-MOP024

About •

paper received ※ 20 June 2019 paper accepted ※ 30 June 2019 issue date ※ 14 August 2019

Export •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

MOP025

Cavity Cut-out Studies of a 1.3 GHz Single-cell Cavity After a Failed Nitrogen Infusion Process

87

M. Wenskat, C. Bate, T.F. Keller, D. Reschke
DESY, Hamburg, Germany
C. Bate
University of Hamburg, Hamburg, Germany
A. Jeromin
DESY Nanolab, FS-NL, Hamburg, Germany
J. Knobloch, F. Kramer, O. Kugeler, J.M. Köszegi
HZB, Berlin, Germany
J. Knobloch
University of Siegen, Siegen, Germany

Funding: This work was supported by the Helmholtz Association within the topic Accelerator Research and Development (ARD) of the Matter and Technologies (MT) Program and by the BMBF under the research grant 05H18GURB1.
R&D on the nitrogen infusion process at DESY produced at the beginning a series of 1.3 GHz single-cell cavities which have shown severe deterioration in the vertical cold test which was completely unexpected and could not be explained. To investigate the reason for the deterioration, one of those cavities was optically inspected and a T- and H-Map test was done in collaboration with HZB. Together with 2nd Sound data, regions of interests were identified and cut from the cavity. Subsequent surface analysis techniques (SEM/EDX, SIMS, PIXE, EBSD, DB-PAS, PALS, XPS) were applied in order to identify the reason for the deterioration. Especially the differences between hot and cold spots as well as quench spots identified by T-Mapping were investigated.

Poster MOP025 [0.975 MB]

DOI •

reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-MOP025

About •

paper received ※ 20 June 2019 paper accepted ※ 29 June 2019 issue date ※ 14 August 2019

Export •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

TUP099

Particulate Sampling and Analysis During Refurbishment of Prototype European XFEL Cryomodule

701

N. Krupka, C. Bate, D. Reschke, S. Saegebarth, M. Schalwat, P. Schilling, S. Sievers
DESY, Hamburg, Germany

Funding: This work was supported by the Helmholtz Association within the topic Accelerator Research and Development (ARD) of the Matter and Tech-nologies (MT) Program.
The cryomodule PXFEL3₁ is one of three prototype cryomodules for the European XFEL. In preparation of the series module assembly it was used for the qualification of infrastructure and personnel at CEA Saclay. After transport and tests at DESY the cryomodule was stored for several years. Last year we decided to refurbish this module with new cavities for the installation in the FLASH accelerator. During the disassembly of the cavity string in the clean room at DESY we took several particulate samples for analysis. Optical and laser optical microscopy give us an insight on the quantity and type of the particulates. We expect to get hints where the particulates come from and how they are transported through the cavity string during transport and operation.

Poster TUP099 [2.599 MB]

DOI •

reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-TUP099

About •

paper received ※ 23 June 2019 paper accepted ※ 03 July 2019 issue date ※ 14 August 2019

Export •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

TUFUA6

Surface Analysis of Niobium After Thermal/Gas Treatments via Samples - Review

A. Dangwal Pandey, T.F. Keller, H. Noei, D. Reschke, J. Schaffran, G.D.L. Semione, V. Vonk, H. Weise, M. Wenskat
DESY, Hamburg, Germany
C. Bate, A. Stierle
University of Hamburg, Hamburg, Germany

Thermal treatments of SRF Nb cavities - including the well-established 120°C bake and the recently reported N-infusion - are shown to improve the cavity performance significantly; however, the underlying physical phenomenon is not fully understood. A short review will be presented on surface characterization of niobium material subjected to various thermal and gas exposure protocols and how the findings correlate with observed SRF properties. Moreover, recent results obtained on single-crystal Nb samples - heated in different vacuum environments and characterised by means of X-ray photoelectron spectroscopy and grazing-incidence X-ray diffraction, electron microscopy, energy dispersive X-ray spectroscopy and time-of-flight secondary ion mass spectroscopy will be discussed.

Slides TUFUA6 [6.968 MB]

Export •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)