MEDSI2023 - List of Authors (Ou, Z.N.)

Paper	Title	Page
TUPYP010	A Novel Coating to Avoid Corrosion Effect and Vibration Coupling Between Eutectic Gallium-Indium Alloy and Heat Sink Metal for X-Ray Optics Cooling
	T. He, M. Li, W.C. Liu, Z.N. Ou, Z.R. Ren, W.F. Sheng, S. Tang, J.L. Yang, H.H. Yu, X.M. Zhang IHEP, Beijing, People’s Republic of China T. He, M. Li, W.C. Liu, W.F. Sheng, S. Tang, J.L. Yang, H.H. Yu, X.M. Zhang University of Chinese Academy of Sciences, Beijing, People’s Republic of China
	Although the vibration decoupling method based on eutectic gallium-indium (EGaIn) alloy performs excellent in suppressing parasitic vibration caused by the cooling medium and pipes of X-ray optics, the corrosion of EGaIn alloy to the heat sink metal still results in the solidification and the vibration decoupling failure. A novel anti-corrosion coating based on tungsten(W) is proposed. Through the analysis of the micromorphology and the chemical composition after heating for 36 hours at 250°C, there is no obvious evidence that W is corroded which is more effective than the widely used coating of nickle(Ni). And the W coating by using magnetron sputtering has been implemented for feasibility validation. Its corrosion resistance mechanism has also been fully analyzed. Besides, finite element analysis on the differences of vibration decoupling after applying W coatings and Ni coatings are also carried out and discussed. W is proved to be a considerable coating for vibration decoupling to face up to the challenge of the ultra-high requirements of high stability (~10nrad RMS), high surface shape accuracy (¿50nrad RMS) in diffraction-limited storage ring light source.
	Poster TUPYP010 [10.504 MB]
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TUPYP023	Design of a Long Versatile Detector Tube System for Pink Beam Small-Angle X-Ray Scattering (SAXS) Beamline at HEPS	64
	Z.Q. Cui, G. Mo, Z.N. Ou, S. Tang, X. Xing, J.C. Zhang IHEP, Beijing, People’s Republic of China
	The long versatile detector tube system for small-angle X-ray scattering meets the experimental conditions of -5-50° wide-angle X-ray scattering (WAXS), 0.04-6° small-angle X-ray scattering (SAXS) and 0.001-0.1° ultra-small-angle X-ray scattering (USAXS), record the same change process of the same sample, and obtain comprehensive structural information of atomic size, nanometer size and micron size, which can be applied to nanomaterials, mesoporous materials, biological macromolecules, polymers and other fields. The size of the tube system is 26760×1945×2565 mm,and consists of four parts: WAXS device, SAXS device, USAXS device and vacuum chamber. The vacuum chamber is assembled by connecting and assembling parts such as thick and fine pipes, bellows, heads and vacuum valves, with a length of 13775 mm and an inner diameter of 1500mm. The thin pipe is 7740 mm long and has an inner diameter of 300 mm. The design scheme of the tube system is committed to ensuring that the distance between the SAXS detector and the sample is continuously adjustable within the range of 1-13.5 m in vacuum environment, and the straightness of the 13840 mm long track of the SAXS device is better than 1 mm.
	Poster TUPYP023 [1.737 MB]
DOI •	reference for this paper ※ doi:10.18429/JACoW-MEDSI2023-TUPYP023
About •	Received ※ 02 November 2023 — Revised ※ 03 November 2023 — Accepted ※ 09 November 2023 — Issued ※ 25 January 2024
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TUPYP037	Mechanical Design of Multilayer Kirkpatrick-Baez (KB) Mirror System for Structural Dynamics Beamline (SDB) at High Energy Photon Source (HEPS)	82
	R.Y. Liao, L. Gao, Z.N. Ou, S. Tang, H.H. Yu, B.B. Zhang IHEP, Bejing, People’s Republic of China
	SDB aims in-situ real-time diagnosis in dynamic compression science and additive manufacturing. Nano-experimental environment requires highly multilayer KB mirror system in thermal deformation and stability of mechanism. This paper illustrates the KB cooling scheme and mechanical design. Only using variable-length water cooling to control the temperature and thermal deformation of mirror has limitations here. First, the installation of cooling system should be non-contact so that the surface shape can be sophisticatedly controlled without deformation of chucking power. Second, the distance between the HKB and the sample stage is too small to arrange the cooling pipe. Third, the KB mirror has multi-dimensional attitude adjustment. Cu water cooling pipe would be dragged with adjustment thus it has to be bent for motion decoupling, which occupies considerable space. Thus, the Cu cooling block and water cooling pipe are connected by copper braid. Eutectic Gallium-Indium fills a 100 ¿m gap between the cooling block and KB mirror to avoid chunking power deformation. Finally, the structural stability and chamber sealability is analyzed.
	Poster TUPYP037 [1.234 MB]
DOI •	reference for this paper ※ doi:10.18429/JACoW-MEDSI2023-TUPYP037
About •	Received ※ 24 October 2023 — Revised ※ 04 November 2023 — Accepted ※ 08 November 2023 — Issued ※ 12 April 2024
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TUPYP040	Experimental Setup Design of Hard X-ray Coherent Scattering (HXCS) Beamline at HEPS
	Z.N. Ou, R.Y. Liao, S. Tang, X. Wang, H.H. Yu, L. Zhou IHEP, People’s Republic of China
	The HXCS is a dedicated coherent beamline of the High Energy Photon Source (HEPS). The experimental setup of the endstation mainly includes two devices: CDI/WAXS XPCS and SAXS XPCS. To achieve high stability requirements, the CDI/WAXS XPCS device use a nano-focusing AKB mirrors system, which will focus hard x-rays to a focal spot as small as 100 nm with a small working distance of 64 mm. In the narrow working distance, AKB mirror chamber and sample chamber are designed as a unit but separated from the middle. And the device is designed with two sets of switchable sample table, in order to flexibly carry out four coherent techniques. Due to high stability, the CDI/WAXS XPCS device is stringent designed for high stiffness, high temperature stability and metrology. Besides, the other important equipments of the beamline include a 1.5m WAXS tube and a 14m SAXS tube. For high-resolution applications, the WAXS tube can be rotated around the sample in the horizontal and vertical plane by 45°and the SAXS tube can adjust distance and angulation. At present, the whole experimental setup is designed according to the fine mechanical design which can meet the experimental requirements.
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WEPPP016	Mechanical Design of XRS & RIXS Multi-Functional Spectrometer at the High Energy Photon Source	178
	J.C. Zhang, Z.Y. Guo, X. Jia, S.X. Jin, Z.N. Ou, W.F. Sheng, S. Tang, R.Z. Xu, W. Xu, Y.J. Zhang IHEP, Beijing, People’s Republic of China
	The integration of an X-ray Raman spectroscopy (XRS) spectrometer and a Resonant Inelastic X-ray scattering (RIXS) spectrometer at HEPS is described. The XRS has 6 regular modular groups and 1 high resolution modular group. In total 90 pieces of spherically bent analyzer crystals are mounted in low vacuum chambers with pressure lower than 100Pa. On the other hand, the RIXS spectrometer possesses one spherically bent analyzer crystal configured in Rowland geometry whose diameter is changeable from 1m to 2m. The scattering X-ray photons transport mostly in helium chamber to reduce absorption by air. The RIXS and the high resolution module can be exchanged when needed. Six air feet are set under the granite plate to unload the weight when the heavy spectrometer is aligned. The natural frequency and statics of the main granite rack were analyzed and optimized to maintain high stability for the HEPS-ID33 beamline at the 4th generation source. A type of compact and cost-effective adjustment gadget for the crystals was designed and fabricated. Economic solutions in selection of motors and sensors and other aspects were adopted for building the large spectrometer like this.
DOI •	reference for this paper ※ doi:10.18429/JACoW-MEDSI2023-WEPPP016
About •	Received ※ 02 November 2023 — Revised ※ 06 November 2023 — Accepted ※ 09 November 2023 — Issued ※ 11 April 2024
Cite •	reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

THOAM04	Overall Progress on Development of X-ray Optics Mechanical Systems at High Energy Photon Source (HEPS)	252
	S. Tang, Y.H. Dong, X.H. Kuang, M. Li, H. Liang, R.Y. Liao, L.H. Ma, Z.N. Ou, H. Qian, Z.R. Ren, W.F. Sheng, J. Wang, R.Z. Xu, H.H. Yu IHEP, People’s Republic of China
	Funding: This work is supported by the project of High Energy Photon Source (HEPS). High Energy Photon Source (HEPS) regarded as a new 4th generation synchrotron radiation facility, is under construction in a virgin green field in Beijing, China. The X-ray optics/mirror mechanical systems (MMS) play an important role, which would be expected to be designed carefully and rigidly for the extremely stable performance requirement of HEPS. In addition, there are indeed big challenges due to so many types of mirror systems, such as white beam mirror (WBM), harmonic suppression mirror (HSM), combined deflecting mirror (CDM), bending mirror, Nano-KB, and the transfocator of Compound refractive lens (CRLs), etc. Therefore, overall progress on design and maunfacturing of the MMS is introduced, in which a promoting strategy and generic mirror mechanical system as a key technology is presented and developed for the project of HEPS. Furthermore, ultra-stable structucture, multi-DOF precision positioning, Eutectic Galium Indium (E-GaIn)-based vibration-decoupling watercooling, clamping, and bending have always been prior designs and considerations. Shanzhi Tang, Weifan Sheng, Jianye Wang, et al, Overall progress on the design of mirror mechanical systems at High Energy Photon Source (HEPS), SRI2021, Hamburg Germany, 2022. POSTER
	Slides THOAM04 [2.328 MB]
DOI •	reference for this paper ※ doi:10.18429/JACoW-MEDSI2023-THOAM04
About •	Received ※ 30 October 2023 — Revised ※ 05 November 2023 — Accepted ※ 10 November 2023 — Issued ※ 18 July 2024
Cite •	reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

THPPP022	A compact direct measurement method for relative positioning of KB mirrors nano-experimental apparatus based on grating interferometers
	S. Tang, T. He, M. Li, R.Y. Liao, Z.N. Ou, W.F. Sheng, Y. Tao, H.H. Yu, L. Zhou IHEP, People’s Republic of China T. He University of Chinese Academy of Sciences, Beijing, People’s Republic of China H.H. Yu UCAS, Beijing, People’s Republic of China
	Funding: This work is supported by the project of High Energy Photon Source (HEPS). Positioning measurement is regraded as an effective way for the position compensation and feedback of nano-experimental apparatus. However, it usually suffers many restrictions from the complicated applied occasion of a typical performance beamline for next-generation synchrotron radiation light source. To deal with the problem, a compact direct measurement method based on grating interferometers is presented. The principle, configuration, experiment are designed and implemented for the verification of the feasibility. It performs a high resolution in orthogonal/lateral direction relative to laser beam, which can overcome an infeasible shortage of a typical interferometer for direct lateral positioning. So, it is used for positioning measurement & compensation between KB mirrors and nano-stages of a sample for the experiments of CDI, bragg-CDI, pytchograph, XPCS, etc. Compared with the existed methods, huge frame, two vacuum chambers restriction, multi-axis interferometer and benchmark relay are avoided for the compact system by using proposed method.
	Poster THPPP022 [2.006 MB]
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Paper

Title

Page

TUPYP010

A Novel Coating to Avoid Corrosion Effect and Vibration Coupling Between Eutectic Gallium-Indium Alloy and Heat Sink Metal for X-Ray Optics Cooling

T. He, M. Li, W.C. Liu, Z.N. Ou, Z.R. Ren, W.F. Sheng, S. Tang, J.L. Yang, H.H. Yu, X.M. Zhang
IHEP, Beijing, People’s Republic of China
T. He, M. Li, W.C. Liu, W.F. Sheng, S. Tang, J.L. Yang, H.H. Yu, X.M. Zhang
University of Chinese Academy of Sciences, Beijing, People’s Republic of China

Although the vibration decoupling method based on eutectic gallium-indium (EGaIn) alloy performs excellent in suppressing parasitic vibration caused by the cooling medium and pipes of X-ray optics, the corrosion of EGaIn alloy to the heat sink metal still results in the solidification and the vibration decoupling failure. A novel anti-corrosion coating based on tungsten(W) is proposed. Through the analysis of the micromorphology and the chemical composition after heating for 36 hours at 250°C, there is no obvious evidence that W is corroded which is more effective than the widely used coating of nickle(Ni). And the W coating by using magnetron sputtering has been implemented for feasibility validation. Its corrosion resistance mechanism has also been fully analyzed. Besides, finite element analysis on the differences of vibration decoupling after applying W coatings and Ni coatings are also carried out and discussed. W is proved to be a considerable coating for vibration decoupling to face up to the challenge of the ultra-high requirements of high stability (~10nrad RMS), high surface shape accuracy (¿50nrad RMS) in diffraction-limited storage ring light source.

Poster TUPYP010 [10.504 MB]

Cite •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

TUPYP023

Design of a Long Versatile Detector Tube System for Pink Beam Small-Angle X-Ray Scattering (SAXS) Beamline at HEPS

64

Z.Q. Cui, G. Mo, Z.N. Ou, S. Tang, X. Xing, J.C. Zhang
IHEP, Beijing, People’s Republic of China

The long versatile detector tube system for small-angle X-ray scattering meets the experimental conditions of -5-50° wide-angle X-ray scattering (WAXS), 0.04-6° small-angle X-ray scattering (SAXS) and 0.001-0.1° ultra-small-angle X-ray scattering (USAXS), record the same change process of the same sample, and obtain comprehensive structural information of atomic size, nanometer size and micron size, which can be applied to nanomaterials, mesoporous materials, biological macromolecules, polymers and other fields. The size of the tube system is 26760×1945×2565 mm,and consists of four parts: WAXS device, SAXS device, USAXS device and vacuum chamber. The vacuum chamber is assembled by connecting and assembling parts such as thick and fine pipes, bellows, heads and vacuum valves, with a length of 13775 mm and an inner diameter of 1500mm. The thin pipe is 7740 mm long and has an inner diameter of 300 mm. The design scheme of the tube system is committed to ensuring that the distance between the SAXS detector and the sample is continuously adjustable within the range of 1-13.5 m in vacuum environment, and the straightness of the 13840 mm long track of the SAXS device is better than 1 mm.

Poster TUPYP023 [1.737 MB]

DOI •

reference for this paper ※ doi:10.18429/JACoW-MEDSI2023-TUPYP023

About •

Received ※ 02 November 2023 — Revised ※ 03 November 2023 — Accepted ※ 09 November 2023 — Issued ※ 25 January 2024

Cite •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

TUPYP037

Mechanical Design of Multilayer Kirkpatrick-Baez (KB) Mirror System for Structural Dynamics Beamline (SDB) at High Energy Photon Source (HEPS)

82

R.Y. Liao, L. Gao, Z.N. Ou, S. Tang, H.H. Yu, B.B. Zhang
IHEP, Bejing, People’s Republic of China

SDB aims in-situ real-time diagnosis in dynamic compression science and additive manufacturing. Nano-experimental environment requires highly multilayer KB mirror system in thermal deformation and stability of mechanism. This paper illustrates the KB cooling scheme and mechanical design. Only using variable-length water cooling to control the temperature and thermal deformation of mirror has limitations here. First, the installation of cooling system should be non-contact so that the surface shape can be sophisticatedly controlled without deformation of chucking power. Second, the distance between the HKB and the sample stage is too small to arrange the cooling pipe. Third, the KB mirror has multi-dimensional attitude adjustment. Cu water cooling pipe would be dragged with adjustment thus it has to be bent for motion decoupling, which occupies considerable space. Thus, the Cu cooling block and water cooling pipe are connected by copper braid. Eutectic Gallium-Indium fills a 100 ¿m gap between the cooling block and KB mirror to avoid chunking power deformation. Finally, the structural stability and chamber sealability is analyzed.

Poster TUPYP037 [1.234 MB]

DOI •

reference for this paper ※ doi:10.18429/JACoW-MEDSI2023-TUPYP037

About •

Received ※ 24 October 2023 — Revised ※ 04 November 2023 — Accepted ※ 08 November 2023 — Issued ※ 12 April 2024

Cite •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

TUPYP040

Experimental Setup Design of Hard X-ray Coherent Scattering (HXCS) Beamline at HEPS

Z.N. Ou, R.Y. Liao, S. Tang, X. Wang, H.H. Yu, L. Zhou
IHEP, People’s Republic of China

The HXCS is a dedicated coherent beamline of the High Energy Photon Source (HEPS). The experimental setup of the endstation mainly includes two devices: CDI/WAXS XPCS and SAXS XPCS. To achieve high stability requirements, the CDI/WAXS XPCS device use a nano-focusing AKB mirrors system, which will focus hard x-rays to a focal spot as small as 100 nm with a small working distance of 64 mm. In the narrow working distance, AKB mirror chamber and sample chamber are designed as a unit but separated from the middle. And the device is designed with two sets of switchable sample table, in order to flexibly carry out four coherent techniques. Due to high stability, the CDI/WAXS XPCS device is stringent designed for high stiffness, high temperature stability and metrology. Besides, the other important equipments of the beamline include a 1.5m WAXS tube and a 14m SAXS tube. For high-resolution applications, the WAXS tube can be rotated around the sample in the horizontal and vertical plane by 45°and the SAXS tube can adjust distance and angulation. At present, the whole experimental setup is designed according to the fine mechanical design which can meet the experimental requirements.

Cite •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

WEPPP016

Mechanical Design of XRS & RIXS Multi-Functional Spectrometer at the High Energy Photon Source

178

J.C. Zhang, Z.Y. Guo, X. Jia, S.X. Jin, Z.N. Ou, W.F. Sheng, S. Tang, R.Z. Xu, W. Xu, Y.J. Zhang
IHEP, Beijing, People’s Republic of China

The integration of an X-ray Raman spectroscopy (XRS) spectrometer and a Resonant Inelastic X-ray scattering (RIXS) spectrometer at HEPS is described. The XRS has 6 regular modular groups and 1 high resolution modular group. In total 90 pieces of spherically bent analyzer crystals are mounted in low vacuum chambers with pressure lower than 100Pa. On the other hand, the RIXS spectrometer possesses one spherically bent analyzer crystal configured in Rowland geometry whose diameter is changeable from 1m to 2m. The scattering X-ray photons transport mostly in helium chamber to reduce absorption by air. The RIXS and the high resolution module can be exchanged when needed. Six air feet are set under the granite plate to unload the weight when the heavy spectrometer is aligned. The natural frequency and statics of the main granite rack were analyzed and optimized to maintain high stability for the HEPS-ID33 beamline at the 4th generation source. A type of compact and cost-effective adjustment gadget for the crystals was designed and fabricated. Economic solutions in selection of motors and sensors and other aspects were adopted for building the large spectrometer like this.

DOI •

reference for this paper ※ doi:10.18429/JACoW-MEDSI2023-WEPPP016

About •

Received ※ 02 November 2023 — Revised ※ 06 November 2023 — Accepted ※ 09 November 2023 — Issued ※ 11 April 2024

Cite •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

THOAM04

Overall Progress on Development of X-ray Optics Mechanical Systems at High Energy Photon Source (HEPS)

252

S. Tang, Y.H. Dong, X.H. Kuang, M. Li, H. Liang, R.Y. Liao, L.H. Ma, Z.N. Ou, H. Qian, Z.R. Ren, W.F. Sheng, J. Wang, R.Z. Xu, H.H. Yu
IHEP, People’s Republic of China

Funding: This work is supported by the project of High Energy Photon Source (HEPS).
High Energy Photon Source (HEPS) regarded as a new 4th generation synchrotron radiation facility, is under construction in a virgin green field in Beijing, China. The X-ray optics/mirror mechanical systems (MMS) play an important role, which would be expected to be designed carefully and rigidly for the extremely stable performance requirement of HEPS. In addition, there are indeed big challenges due to so many types of mirror systems, such as white beam mirror (WBM), harmonic suppression mirror (HSM), combined deflecting mirror (CDM), bending mirror, Nano-KB, and the transfocator of Compound refractive lens (CRLs), etc. Therefore, overall progress on design and maunfacturing of the MMS is introduced, in which a promoting strategy and generic mirror mechanical system as a key technology is presented and developed for the project of HEPS. Furthermore, ultra-stable structucture, multi-DOF precision positioning, Eutectic Galium Indium (E-GaIn)-based vibration-decoupling watercooling, clamping, and bending have always been prior designs and considerations.
Shanzhi Tang, Weifan Sheng, Jianye Wang, et al, Overall progress on the design of mirror mechanical systems at High Energy Photon Source (HEPS), SRI2021, Hamburg Germany, 2022. POSTER

Slides THOAM04 [2.328 MB]

DOI •

reference for this paper ※ doi:10.18429/JACoW-MEDSI2023-THOAM04

About •

Received ※ 30 October 2023 — Revised ※ 05 November 2023 — Accepted ※ 10 November 2023 — Issued ※ 18 July 2024

Cite •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

THPPP022

A compact direct measurement method for relative positioning of KB mirrors nano-experimental apparatus based on grating interferometers

S. Tang, T. He, M. Li, R.Y. Liao, Z.N. Ou, W.F. Sheng, Y. Tao, H.H. Yu, L. Zhou
IHEP, People’s Republic of China
T. He
University of Chinese Academy of Sciences, Beijing, People’s Republic of China
H.H. Yu
UCAS, Beijing, People’s Republic of China

Funding: This work is supported by the project of High Energy Photon Source (HEPS).
Positioning measurement is regraded as an effective way for the position compensation and feedback of nano-experimental apparatus. However, it usually suffers many restrictions from the complicated applied occasion of a typical performance beamline for next-generation synchrotron radiation light source. To deal with the problem, a compact direct measurement method based on grating interferometers is presented. The principle, configuration, experiment are designed and implemented for the verification of the feasibility. It performs a high resolution in orthogonal/lateral direction relative to laser beam, which can overcome an infeasible shortage of a typical interferometer for direct lateral positioning. So, it is used for positioning measurement & compensation between KB mirrors and nano-stages of a sample for the experiments of CDI, bragg-CDI, pytchograph, XPCS, etc. Compared with the existed methods, huge frame, two vacuum chambers restriction, multi-axis interferometer and benchmark relay are avoided for the compact system by using proposed method.

Poster THPPP022 [2.006 MB]

Cite •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)