Author: Maniscalco, J.T.
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MOBA08 Niobium Impurity-Doping Studies at Cornell and CM Cool-Down Dynamic Effect on Q0 55
 
  • M. Liepe, B. Clasby, R.G. Eichhorn, B. Elmore, F. Furuta, G.M. Ge, D. Gonnella, T. Gruber, D.L. Hall, G.H. Hoffstaetter, J.J. Kaufman, P.N. Koufalis, J.T. Maniscalco, T.I. O'Connell, P. Quigley, D.M. Sabol, J. Sears, E.N. Smith, V. Veshcherevich
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
 
  As part of a multi-laboratory research initiative on high Q0 niobium cavities for LCLS-II and other future CW SRF accelerators, Cornell has conducted an extensive research program during the last two years on impurity-doping of niobium cavities and related material characterization. Here we give an overview of these activities, and present results from single-cell studies, from vertical performance testing of nitrogen-doped nine-cell cavities, and from cryomodule testing of nitrogen-doped nine-cell cavities.  
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MOPB004 Understanding the Field Dependence of the Surface Resistance in Nitrogen-Doped Cavities 74
 
  • P.N. Koufalis, D. Gonnella, M. Liepe, J.T. Maniscalco, I. Packtor
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
 
  Funding: NSF Grant PHYS-1416318
An important limiting factor in the performance of superconducting radio frequency (SRF) cavities in medium and high field gradients is the intrinsic quality factor and, thus, the surface resistance of the cavity. The exact dependence of the surface resistance on the magnitude of the RF field is not well understood. We present an analysis of experimental data of LT1-3 and LT1-4, 1.3 GHz single-cell nitrogen-doped cavities prepared and tested at Cornell. Most interestingly, the cavities display anti-Q slopes in the medium-field region (i.e. Rs decreases with increasing accelerating field). We extract the temperature dependent surface resistances of the cavities, analyze field dependencies, and compare with theoretical predictions. These comparisons and analyses provide new insights into the field dependence of the surface resistance and improve our understanding of the mechanisms behind the effect.
 
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MOPB005 Developing a Setup to Measure Field Dependence of BCS Surface Resistance 77
 
  • J.T. Maniscalco, M. Liepe
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
 
  Funding: NSF/DOE
The temperature-dependent part of the microwave surface resistance of superconducting radio-frequency (SRF) cavities has been shown experimentally to depend on the strength of the applied magnetic surface field. Several theories have recently been proposed to describe this phenomenon. In this paper we present work on the development of a microwave cavity setup for measuring the field-dependence with an applied DC magnetic field.
 
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MOPB006 Hc2 Measurements of Superconductors 79
 
  • J.T. Maniscalco, D. Gonnella, D.L. Hall, M. Liepe, E.N. Smith
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
 
  Funding: NSF/DOE
Recently, Cornell has improved a method for extracting the upper critical field Hc2 of a thin-film superconductor using four-point resistivity measurements. In the field of superconducting radio-frequency accelerators (SRF), novel materials and processes such as nitrogen-doped niobium and Nb3Sn may allow for improved SRF performance and cost efficiency over traditional niobium. In this paper we present updated results on Hc2 measurements for Nb3Sn, as well as results for niobium prepared with an 800 C bake. We also extract important material properties from these measurements, such as the Ginzburg Landau parameter, the mean free path, and coherence length, which are critical for determining SRF performance.
 
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MOPB033 LCLS-II SRF Cavity Processing Protocol Development and Baseline Cavity Performance Demonstration 159
 
  • M. Liepe, P. Bishop, H. Conklin, R.G. Eichhorn, F. Furuta, G.M. Ge, D. Gonnella, T. Gruber, D.L. Hall, G.H. Hoffstaetter, J.J. Kaufman, G. Kulina, J.T. Maniscalco, T.I. O'Connell, P. Quigley, D.M. Sabol, J. Sears, V. Veshcherevich
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
  • M. Checchin, A.C. Crawford, A. Grassellino, C.J. Grimm, A. Hocker, M. Martinello, O.S. Melnychuk, J.P. Ozelis, A. Romanenko, A.M. Rowe, D.A. Sergatskov, W.M. Soyars, R.P. Stanek, G. Wu
    Fermilab, Batavia, Illinois, USA
  • E. Daly, G.K. Davis, M.A. Drury, J.F. Fischer, A.D. Palczewski, C.E. Reece
    JLab, Newport News, Virginia, USA
  • M.C. Ross
    SLAC, Menlo Park, California, USA
 
  Funding: Work supported, in part, by the US DOE and the LCLS-II Project under U.S. DOE Contract No. DE-AC05-06OR23177 and DE-AC02-76SF00515.
The ”Linac Coherent Light Source-II” Project will construct a 4 GeV CW superconducting RF linac in the first kilometer of the existing SLAC linac tunnel. The baseline design calls for 280 1.3 GHz nine-cell cavities with an average intrinsic quality factor Q0 of 2.7·1010 at 2K and 16 MV/m accelerating gradient. The LCLS-II high Q0 cavity treatment protocol utilizes the reduction in BCS surface resistance by nitrogen doping of the RF surface layer, which was discovered originally at FNAL. Cornell University, FNAL, and TJNAF conducted a joint high Q0 R&D program with the goal of (a) exploring the robustness of the N-doping technique and establishing the LCLS-II cavity high Q0 processing protocol suitable for production use, and (b) demonstrating that this process can reliably achieve LCLS-II cavity specification in a production acceptance testing setting. In this paper we describe the LCLS-II cavity protocol and analyze combined cavity performance data from both vertical and horizontal testing at the three partner labs, which clearly shows that LCLS-II specifications were met, and thus demonstrates readiness for LCLS-II cavity production.
 
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MOPB041 Cryomodule Testing of Nitrogen-Doped Cavities 182
 
  • D. Gonnella, B. Clasby, R.G. Eichhorn, B. Elmore, F. Furuta, G.M. Ge, D.L. Hall, Y. He, G.H. Hoffstaetter, J.J. Kaufman, P.N. Koufalis, M. Liepe, J.T. Maniscalco, T.I. O'Connell, P. Quigley, D.M. Sabol, E.N. Smith, V. Veshcherevich
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
  • A. Grassellino, C.J. Grimm, J.P. Holzbauer, O.S. Melnychuk, Y.M. Pischalnikov, A. Romanenko, W. Schappert, D.A. Sergatskov
    Fermilab, Batavia, Illinois, USA
  • A.D. Palczewski, C.E. Reece
    JLab, Newport News, Virginia, USA
 
  Funding: DOE and the LCLS-II High Q Project
The Linac Coherent Light Source-II (LCLS-II) is a new FEL x-ray source that is planned to be constructed in the existing SLAC tunnel. In order to meet the required high Q0 specification of 2.7x1010 at 2 K and 16 MV/m, nitrogen-doping has been proposed as a preparation method for the SRF cavities in the linac. In order to test the feasibility of these goals, four nitrogen-doped cavities have been tested at Cornell in the Horizontal Test Cryomodule (HTC) in five separate tests. The first three tests consisted of cavities assembled in the HTC with high Q input coupler. The fourth test used the same cavity as the third but with the prototype high power LCLS-II coupler installed. Finally, the fifth test used a high power LCLS-II coupler, cavity tuner, and HOM antennas. Here we report on the results from these tests along with a systematic analysis of change in performance due to the various steps in preparing and assembling LCLS-II cavities for cryomodule operation. These results represent one of the final steps to demonstrate readiness for full prototype cryomodule assembly for LCLS-II.
 
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MOPB042 Fundamental Studies on Doped SRF Cavities 187
 
  • D. Gonnella, T. Gruber, J.J. Kaufman, P.N. Koufalis, M. Liepe, J.T. Maniscalco, B. Yu
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
 
  Funding: NSF
Recently, doping with nitrogen has been demonstrated to help SRF cavities reach significantly higher intrinsic quality factors than with standard procedures. However, the quench fields of these cavities have also been shown to be frequently reduced. Here we report on fundamental studies of doped cavities, investigating the source of reduced quench field and exploring alternative dopants. We have focused on studying the quench of nitrogen-doped cavities with temperature mapping and measurements of the flux penetration field using pulsed power to investigate maximum fields in nitrogen doped cavities. We also report on studies of cavities doped with other gases such as helium. These studies have enabled us to shed light on the mechanisms behind the higher Q and lower quench fields that have been observed in cavities doped with impurities.
 
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TUBA04 Nb3Sn Cavities: Material Characterization and Coating Process Optimization 501
 
  • D.L. Hall, T. Gruber, J.J. Kaufman, M. Liepe, J.T. Maniscalco, S. Posen, B. Yu
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
  • Th. Proslier
    ANL, Argonne, Illinois, USA
 
  Funding: Work supported by DOE grant DE-SC0008431 and NSF grant PHY-141638. Use of CCMR via NSF MRSEC program (DMR-1120296)
Recent progress on vapour diffusion coated Nb3Sn SRF cavities makes this material a very promising alternative for CW medium field SRF applications. In this paper we report on several systematic studies to determine the sources currently limiting the performance of Nb3Sn cavities to determine improved coating parameters to overcome these limitations. These include a detailed study of the sensitivity of Nb3Sn to trapped ambient magnetic flux, a first measurement of the field dependence of the energy gap in Nb3Sn and detailed measurements of the stoichiometry of the obtained Nb3Sn coatings with synchrotron x-ray diffraction and STEM. Initial results from a study on the impact of the coating process parameters on energy gap, Q-slope, and residual resistance, show clear dependencies, and thus directions for process optimization.
 
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TUPB030 Recent Results from the Cornell Sample Host Cavity 626
 
  • J.T. Maniscalco, B. Clasby, T. Gruber, D.L. Hall, M. Liepe
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
 
  Funding: DOE/NSF
Many novel materials are under investigation for the future of superconducting radio-frequency accelerators (SRF). In particular, thin-film materials such as Nb3Sn, NbN, SIS multilayers, and also thin-film niobium on copper, may offer improvements in cost efficiency and RF performance over the standard niobium cavities. To avoid the difficulties of depositing thin films on full cavities, Cornell has developed a TE-mode sample host cavity which allows for RF measurements of large, flat samples at fields up to and over 100 mT. We present recent performance results from the cavity, reaching record high fields and quality factor using a niobium calibration plate. We also discuss plans for future collaborations.
 
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TUPB045 Surface Analysis and Material Property Studies of Nb3Sn on Niobium for Use in SRF Cavities 665
 
  • D.L. Hall, H. Conklin, T. Gruber, J.J. Kaufman, M. Liepe, J.T. Maniscalco, B. Yu
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
  • Th. Proslier
    ANL, Argonne, Illinois, USA
 
  Funding: Work supported by DOE grant DE-SC0008431 and NSF grant PHY-141638. Use of CCMR via NSF MRSEC program (DMR-1120296)
Studies of superconducting Nb3Sn cavities and samples at Cornell University and Argonne National Lab have shown that current state-of-the-art Nb3Sn cavities are limited by material properties and imperfections. In particular, the presence of regions within the Nb3Sn layer that are deficient in tin are suspected to be the cause of the lower than expected peak accelerating gradient. In this paper we present results from a material study of the Nb3Sn layer fabricated using the vapour deposition method, with data collected using AFM, SEM, TEM, EDX, and XRD methods as well as with pulsed RF testing.
 
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