Author: Trofimova, O.
Paper Title Page
TUP030 Automation of Particulate Characterization 477
 
  • J.K. Spradlin, C.E. Reece, O. Trofimova, A-M. Valente-Feliciano
    JLab, Newport News, Virginia, USA
 
  Funding: Notice: This manuscript has been authored by Jefferson Science Associates, LLC under Contract No. DE-AC05-06OR23177 with the U.S. Department of Energy.
Foreign particles residing on the field carrying surface of accelerator cavities are a known mechanism for field emission. Developing the methods and tools for collecting and characterizing particles found in an accelerator enables process development towards field emission free SRF cavities. Methods are presented for sampling assemblies, components, processes, and environmental conditions utilizing forensic techniques with specialized tooling. Sampling activities to date have produced an inventory of over 850 GSR spindles. Traditional SEM + EDS analysis of this volume of spindles is challenged by labor investment, spindle sampling methods, and the subsequent data pipeline which ultimately results in a statically inadequate dataset for any particulate distribution characterization. A complete systematic analysis of the spindles is enabled by third party software controlling SEM automation for EDS data acquisition. Details of spindle creation, collection equipment, component sampling, automating particle assessment, and data analysis used to characterize samples from beamline elements in CEBAF are presented.
 
poster icon Poster TUP030 [3.257 MB]  
DOI • reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-TUP030  
About • paper received ※ 21 June 2019       paper accepted ※ 14 August 2019       issue date ※ 14 August 2019  
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WETEB2 Identifying Specific Cryomodule and Cleanroom Particulate Contamination: Understanding Legacy Issues and Providing New Feedback Standards 758
 
  • C.E. Reece, J.K. Spradlin, O. Trofimova, A-M. Valente-Feliciano
    JLab, Newport News, Virginia, USA
 
  Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177.
While the techniques used to provide "UHV clean" and "particle-free" beamline components, including SRF cavities, continue to evolve, "real-world" operating machines must deal with actual accumulated and latent contamination issues that produce non-trivial cryogenic heatload, radiation, activation, and degradation via field emission. We have developed a standardized and automated particulate contamination assay method for use in characterizing particulates found on beamline components and in cleanroom assembly environments. We present results from using this system to analyze samples taken from reworked cryomodules from CEBAF. Particle sizes are much larger than anticipated. Utility for feedback on sources to enable improved source reduction is explored.
 
slides icon Slides WETEB2 [13.320 MB]  
DOI • reference for this paper ※ https://doi.org/10.18429/JACoW-SRF2019-WETEB2  
About • paper received ※ 23 June 2019       paper accepted ※ 02 July 2019       issue date ※ 14 August 2019  
Export • reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)