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Eozenou F.

PaperTitlePage
TUP51Electropolishing on Single and MultiI-Cell: COMSOL Modelling247
 
  • M. Bruchon, B. Visentin, F. Eozenou
    CEA-Saclay
 
 In the framework of cavity electropolishing improvement, modelling allows evaluating some parameters not easily accessible by experiments and can also help us to guide them. At CEA Saclay, COMSOL software is used to model electropolishing of cavity in two dimensions. First, single-cell electropolishing with different shapes (TESLA, ILC Low Loss (LLILC), ILC Reentrant (REILC) and the optional Half Re-entrant profile [1, 2]) is studied with acid inflow like in our set up. Then some improvements of both outflow and inflow of the acid are considered. This work is extended to TESLA nine-cell cavities in collaboration with KEK to understand if electropolishing process is related to some misunderstood RF performances [3, 4]. 
TUP69Optimization of Baking Parameters for Electropolished Niobium Superconducting Cavities304
 
  • B. Visentin, Y. Gasser, M. Bruchon, F. Eozenou, J. P. Charrier
    CEA-Saclay
  • D. Reschke, A. Brinkmann
    DESY Hamburg
 
 High gradients, on bulk niobium cavities, can only be reached after an imperative baking at low temperature to suppress the high field Q-drop. We demonstrate in this paper that the commonly used standard process (under ultra high vacuum at 120 degree C for 48 hours) could be now simplified in terms of duration (3 hours at 145 degree C) and requirement (argon atmosphere instead of vacuum). Some efforts to more reduce duration, down to only one hour, have been undertaken to validate hypothesis and understand baking phenomenon. The next improvement step with the open-ended treatment of cavities in oxygen free atmosphere is underway and it does not seem hard to achieve. This new "fast baking" procedure will be very useful in the XFEL and ILC projects where Nb cavities mass production is required. 
TUP71Parameters Investigation for Niobium Electro-Polishing313
 
  • F. Eozenou, M. Bruchon, J. Gantier
    CEA-Saclay
 
 Electro-polishing (EP) experiments are carried out on niobium samples at Saclay in order to highlight the influence of parameters such as temperature and acids concentrations (hydrofluoric and sulfuric). First results given at the 12th SRF Workshop have been completed. The importance of the HF/H2O ratio has been precisely investigated and diluted mixtures have been tested during long time experiments: removal rates, surface states, lifetime of the bath and possible hydrogen contamination will be reported. In addition, some experiments have been carried out with dissolved niobium in fresh mixtures, giving some ideas about mechanisms involved in EP. Furthermore, dissolved salts as well as different acids have been tried as an alternative for hydrofluoric acid use. 
TUP80Single Cell Electro-Polishing at CEA Saclay: First Results343
 
  • F. Eozenou, M. Bruchon, Y. Gasser, Y. Boudigou, B. Visentin, J. P. Charrier, S. Berry, C. Antoine
    CEA-Saclay
  • D. Reschke
    DESY Hamburg
 
 The goal of the Work Package 5.1 of the CARE SRF program is to study electro-polishing (EP) of niobium and thus isolate an ideal set of parameters for 1.3 GHz single cell cavity treatment that should be applied to industry. The more challenging aspect concerns acid composition's optimisation, made of a mixture of hydrofluoric (HF) and sulfuric (H2SO4) acids with possible additional water. Preliminary experiments have been carried out on samples to guide the program on single-cell cavities. In that way, a set-up for horizontal EP has been installed in our laboratory. This set-up has been successfully qualified with the standard recipe used at DESY since the first EP on TESLA-shaped cavity has reached an excellent gradient above 42 MV/m. The search for new parameters makes then sense. Different configurations have been investigated: higher temperature, lower voltage and new acids' concentrations. Dummy cavities have been electropolished with a new mixture: 1vol HF(40w%) - 2vol H2SO4(95w%) - 7vol H2O, (1-2-7) with high water content. Different cavities have also been electro-polished and results including surface aspect, RF measurements and impurities forming will be related.