Author: Palczewski, A.D.
Paper Title Page
MOBA07
Lessons Learned From Nitrogen Doping at JLab - Exploration of Surface Resistance and Quench Field Trade-Offs With Varied Interstitial Atom Diffusion of Niobium Cavity Surfaces  
 
  • A.D. Palczewski, G. Ciovati, P. Dhakal, R.L. Geng, C.E. Reece, H. Tian
    JLab, Newport News, Virginia, USA
 
  Funding: This work is supported by the U.S. Department of Energy, Office of Science, Office of Nuclear Physics under contract DE-AC05-06OR23177 and by the LCLS-II Project under DE-AC02-76SF00515.
Interstitial diffusion of atomic species into the surface of niobium has been found to yield significantly reduced srf surface resistance and lowered quench fields. This talk summarizes systematic efforts to explore the trade-offs of these phenomena with a goal of learning how to maximize Q0 in the 30 MV/m regime. The talk also summarizes N-doped cavity progress at JLab for LCLS-II.
 
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MOPB033 LCLS-II SRF Cavity Processing Protocol Development and Baseline Cavity Performance Demonstration 159
 
  • M. Liepe, P. Bishop, H. Conklin, R.G. Eichhorn, F. Furuta, G.M. Ge, D. Gonnella, T. Gruber, D.L. Hall, G.H. Hoffstaetter, J.J. Kaufman, G. Kulina, J.T. Maniscalco, T.I. O'Connell, P. Quigley, D.M. Sabol, J. Sears, V. Veshcherevich
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
  • M. Checchin, A.C. Crawford, A. Grassellino, C.J. Grimm, A. Hocker, M. Martinello, O.S. Melnychuk, J.P. Ozelis, A. Romanenko, A.M. Rowe, D.A. Sergatskov, W.M. Soyars, R.P. Stanek, G. Wu
    Fermilab, Batavia, Illinois, USA
  • E. Daly, G.K. Davis, M.A. Drury, J.F. Fischer, A.D. Palczewski, C.E. Reece
    JLab, Newport News, Virginia, USA
  • M.C. Ross
    SLAC, Menlo Park, California, USA
 
  Funding: Work supported, in part, by the US DOE and the LCLS-II Project under U.S. DOE Contract No. DE-AC05-06OR23177 and DE-AC02-76SF00515.
The ”Linac Coherent Light Source-II” Project will construct a 4 GeV CW superconducting RF linac in the first kilometer of the existing SLAC linac tunnel. The baseline design calls for 280 1.3 GHz nine-cell cavities with an average intrinsic quality factor Q0 of 2.7·1010 at 2K and 16 MV/m accelerating gradient. The LCLS-II high Q0 cavity treatment protocol utilizes the reduction in BCS surface resistance by nitrogen doping of the RF surface layer, which was discovered originally at FNAL. Cornell University, FNAL, and TJNAF conducted a joint high Q0 R&D program with the goal of (a) exploring the robustness of the N-doping technique and establishing the LCLS-II cavity high Q0 processing protocol suitable for production use, and (b) demonstrating that this process can reliably achieve LCLS-II cavity specification in a production acceptance testing setting. In this paper we describe the LCLS-II cavity protocol and analyze combined cavity performance data from both vertical and horizontal testing at the three partner labs, which clearly shows that LCLS-II specifications were met, and thus demonstrates readiness for LCLS-II cavity production.
 
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MOPB039 Analysis of BCS RF Loss Dependence on N-Doping Protocols 174
 
  • A.D. Palczewski, P. Dhakal, C.E. Reece
    JLab, Newport News, Virginia, USA
 
  Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177 with supplemental funding from the LCLS-II Project U.S. DOE Contract No. DE-AC02-76SF00515.
We present a study on two parallel-path SRF cavities (one large grain and one fine grain, 1.3 GHz) which seeks to explain the correlation between the amount of nitrogen on the inner surface of a “nitrogen doped” SRF cavity and the change in the temperature dependant (packaged into term BCS) RF losses. For each doping/EP, the cavities were tested at multiple temperatures (2.0 K to 1.5 K in 0.1 K steps) to create a Q0 vs. Eacc vs. T matrix which then could be used to extract temperature dependant and independent components. After each test, the cavities were thermally cycled to 120 K and then re-cooled and retested to assess if evidence of hydrogen migration might appear even at a small level. In addition, TD-5 was also tested at fixed low field (Q0 vs. T) to fit standard BCS theory. In parallel, SIMS data was taken on like-treated samples to correlate the amount of nitrogen within the RF surface to the change in the temperature dependant fitting parameter “A”.**
[**] H.Tian et al., contributed to SRF2015.
 
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MOPB040 Performance of Dressed Cavities for the Jefferson Laboratory LCLS-II Prototype Cryomodule - With Comparison to the Pre-Dressed Performance 178
 
  • A.D. Palczewski, G.K. Davis
    JLab, Newport News, Virginia, USA
  • F. Furuta, G.M. Ge, D. Gonnella, M. Liepe
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
 
  Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177 with supplemental funding from the LCLS-II Project U.S. DOE Contract No. DE-AC02-76SF00515.
Initial vertical RF test results and quench studies for six of the eight undressed 9 cell cavities slated for use in the Jefferson laboratory LCLS-II prototype cryomodule were presented at IPAC2015*. For the final string 2 more cavities AES029 and AES030 (work done at Cornell) are being processed and tested for qualification before helium vessel welding. In addition, AES034 (initial R&D treatment) is being reworked with the current production protocol after a surface reset to improve the overall performance. After final qualification all 8 cavities will be welded into helium vessels and equipped with HOM couplers. In this paper we will present the final undressed and dressed vertical RF data comparing the changes in the surface resistance before their installation in the cryomodule string.
*A.D. Palczewski et al. Quench Studies of Six High Temperature Nitrogen Doped 9 Cell Cavities for use in the LCLS-II Prototype Cryo-module at Jefferson Laboratory, Proc. IPAC2015, WEPWI019, 2015.
 
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MOPB041 Cryomodule Testing of Nitrogen-Doped Cavities 182
 
  • D. Gonnella, B. Clasby, R.G. Eichhorn, B. Elmore, F. Furuta, G.M. Ge, D.L. Hall, Y. He, G.H. Hoffstaetter, J.J. Kaufman, P.N. Koufalis, M. Liepe, J.T. Maniscalco, T.I. O'Connell, P. Quigley, D.M. Sabol, E.N. Smith, V. Veshcherevich
    Cornell University (CLASSE), Cornell Laboratory for Accelerator-Based Sciences and Education, Ithaca, New York, USA
  • A. Grassellino, C.J. Grimm, J.P. Holzbauer, O.S. Melnychuk, Y.M. Pischalnikov, A. Romanenko, W. Schappert, D.A. Sergatskov
    Fermilab, Batavia, Illinois, USA
  • A.D. Palczewski, C.E. Reece
    JLab, Newport News, Virginia, USA
 
  Funding: DOE and the LCLS-II High Q Project
The Linac Coherent Light Source-II (LCLS-II) is a new FEL x-ray source that is planned to be constructed in the existing SLAC tunnel. In order to meet the required high Q0 specification of 2.7x1010 at 2 K and 16 MV/m, nitrogen-doping has been proposed as a preparation method for the SRF cavities in the linac. In order to test the feasibility of these goals, four nitrogen-doped cavities have been tested at Cornell in the Horizontal Test Cryomodule (HTC) in five separate tests. The first three tests consisted of cavities assembled in the HTC with high Q input coupler. The fourth test used the same cavity as the third but with the prototype high power LCLS-II coupler installed. Finally, the fifth test used a high power LCLS-II coupler, cavity tuner, and HOM antennas. Here we report on the results from these tests along with a systematic analysis of change in performance due to the various steps in preparing and assembling LCLS-II cavities for cryomodule operation. These results represent one of the final steps to demonstrate readiness for full prototype cryomodule assembly for LCLS-II.
 
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MOPB110 The Transfer of Improved Cavity Processing Protocols to Industry for LCLS-II: N-Doping and Electropolishing 418
 
  • C.E. Reece, F. Marhauser, A.D. Palczewski
    JLab, Newport News, Virginia, USA
 
  Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177 with supplemental funding from the LCLS-II Project U.S. DOE Contract No. DE-AC02-76SF00515.
Based on the R&D efforts of colleagues at FNAL, Cornell, and JLab, the LCLS-II project adopted a modification to the rather standard niobium SRF cavity surface processing protocol that incorporates a high temperature diffusion doping with nitrogen gas. This change was motivated by the resulting higher Q0 and the prospect of significantly lower cryogenic heat load for LCLS-II. JLab is responsible for managing the cavity procurement for the LCLS-II project. The first phase of the procurement action is to transfer the nitrogen-doping protocol to the industrial vendors. We also seek to exploit improvements in understanding of the niobium electropolishing process as part of the production processing of the TESLA-style LCLS-II cavities. We report on the technology transfer activities and progress toward the envisaged performance demonstration of vendor-processed cavities.
 
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